• ASTM C791-12

ASTM C791-12

Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Boron Carbide

ASTM International , 06/01/2012

Publisher: ASTM

File Format: PDF

$43.00$86.00


1.1 These test methods cover procedures for the chemical, mass spectrometric, and spectrochemical analysis of nuclear-grade boron carbide powder and pellets to determine compliance with specifications.

1.2 The analytical procedures appear in the following order:

Sections
Total Carbon by Combustion in an Inductive Furnace and Infrared Measurement 7-16
Total Boron by Titrimetry and ICP OES 17-27
Isotopic Composition by Mass Spectrometry 28-32
Pyrohydrolysis 33-40
Chloride by Constant-Current Coulometry 41-49
Chloride and Fluoride by Ion-Selective Electrode 50-58
Water by Constant-Voltage Coulometry and Weight Loss on Drying 59-62
Metallic Impurities 63 and 64
Soluble Boron by Titrimetry and ICP OES 65-79
Free Carbon by a Coulometric Method 80-89

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