ASTM D3906-03(2013)

1.1This test method covers the determination of relative X-ray diffraction intensities of zeolites having the faujasite crystal structure, including synthetic Y and X zeolites, their modifications such as the various cation exchange forms, and the dealuminized, decationated, and ultrastable forms of Y. These zeolites have cubic symmetry with a unit cell parameter usually within the limits of 24.2 and 25.0 ˚Å (2.42 and 2.50 nm).

1.2The samples include zeolite preparations in the various forms, and catalysts and adsorbents containing these zeolites.

1.3The term “intensity of an X-ray powder diffraction (XRD) peak” is the “integral intensity,” either the area of counts under the peak or the product of the peak height and the peak width.

1.4This test method provides a number that is the ratio of intensity of portions of the XRD pattern of the sample to intensity of the corresponding portion of the pattern of a reference zeolite, NaY. (Laboratories may use a modified Y or X, for example, REY as a secondary standard.) The intensity ratio, expressed as a percentage, is then labeled “% XRD intensity/NaY.”

1.5Under certain conditions such a ratio is the percent zeolite in the sample. These conditions include:

1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.