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ASTM International , 09/01/2017
Publisher: ASTM
File Format: PDF
$54.00$108.00
1.1This procedure covers the determination of selected polyfluorinated compounds (PFCs) in a soil matrix using solvent extraction, filtration, followed by liquid chromatography (LC) and detection with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this method. This method adheres to multiple reaction monitoring (MRM) mass spectrometry. This procedure utilizes a quick extraction and is not intended to generate an exhaustive accounting of the content of PFCs in difficult soil matrices. An exhaustive extraction procedure for polyfluoralkyl substances, such as published by Washington et al.,2 for difficult matrices should be considered when analyzing PFCs.
1.2Units-The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3The Method of Detection Limit3 and Reporting Range4 for the target analytes are listed in Table 1.
Analyte
MDL (ng/kg)
Reporting Limit (ng/kg)
PFTreA
6.76
25-1000
PFTriA
5.26
PFDoA
3.56
PFUnA
2.45
PFDA
5.54
PFOS
18.83
50-1000
PFNA
2.82
PFecHS
2.41
PFOA
6.24
PFHxS
7.75
PFHpA
5.80
PFHxA
15.44
PFBS
6.49
PFPeA
20.93
125-5000
PFBA
22.01
FHEA
199.04
600-20 000
FOEA
258.37
750-20 000
FDEA
137.46
500-20 000
FOUEA
4.85
FhpPa
5.09
FHUEA
3.50
Analyte/Surrogate
LV1
LV2
LV3
LV4
LV5
LV6
LV7
LV8
LV9
PFPeA, PFBA
25
50
100
200
300
400
500
750
1000
PFTreA, PFTriA, PFDoA, PFUnA, PFDA, PFOS, PFNA, PFHxA, PFHpA, PFBS, PFechS, PFOA, PFHxS, FOUEA, FHUEA, FHpPA, MPFBS, MPFHxA, MPFUnA, MPFOA, MPFDA, MPFOS, MPFNA, MPFHxS, MPFBA
5
10
20
40
60
80
150
FHEA, FOEA, FDEA
800
1200
1600
2000
3000
4000
$45.00 $90.00
$41.00 $83.00
$54.00 $108.00
$32.00 $65.00
$34.00 $68.00
$28.00 $56.00
$32.00 $64.00
