• ASTM E352-18

ASTM E352-18

Standard Test Methods for Chemical Analysis of Tool Steels and Other Similar Medium- and High-Alloy Steels

ASTM International , 07/01/2018

Publisher: ASTM

File Format: PDF

$46.00$92.00


1.1These test methods cover the chemical analysis of tool steels and other similar medium- and high-alloy steels having chemical compositions within the following limits:

Element

Composition Range, %

Aluminum

  0.005 to 1.5

Boron

  0.001 to 0.10

Carbon

  0.03  to 2.50

Chromium

  0.10  to 14.0

Cobalt

  0.10  to 14.0

Copper

  0.01  to 2.0

Lead

  0.001 to 0.01

Manganese

  0.10  to 15.00

Molybdenum

  0.01  to 10.00

Nickel

  0.02  to 4.00

Nitrogen

  0.001 to 0.20

Phosphorus

  0.002 to 0.05

Silicon

  0.10  to 2.50

Sulfur

  0.002 to 0.40

Tungsten

  0.01  to 21.00

Vanadium

  0.02  to 5.50

1.2The test methods in this standard are contained in the sections indicated below:

Sections

Carbon, Total, by the Combustion-  Thermal Conductivity Method-  Discontinued 1986

125-135

Carbon, Total, by the Combustion Gravimetric  Method-Discontinued 2012

78-88

Chromium by the Atomic Absorption  Spectrometry Method

(0.006 % to 1.00 %)

174-183

Chromium by the Peroxydisulfate  Oxidation-Titration Method

  (0.10 % to 14.00 %)

184-192

Chromium by the Peroxydisulfate-Oxidation  Titrimetric Method-Discontinued 1980

117-124

Cobalt by the Ion-Exchange-  Potentiometric Titration Method

    (2 % to 14 %) 

52-59

Cobalt by the Nitroso-R-Salt   Spectrophotometric Method

 (0.10 % to 5.0 %) 

60-69

Copper by the Neocuproine   Spectrophotometric Method

 (0.01 % to 2.00 %)

89-98

Copper by the Sulfide Precipitation-  Electrodeposition Gravimetric Method

  (0.01 % to 2.0 %) 

70-77

Lead by the Ion-Exchange-Atomic   Absorption Spectrometry Method

(0.001 % to 0.01 %)

99-108

Manganese by the Periodate   Spectrophotometric Method

 (0.10 % to 5.00 %)

9-18

Molybdenum by the Ion Exchange-  8-Hydroxyquinoline Gravimetric Method 

203-210

Molybdenum by the Thiocyanate Spectrophotometric Method

 (0.01 % to 1.50 %)

162-173

Nickel by the Dimethylglyoxime  Gravimetric Method

(0.1 % to 4.0 %)

144-151

Phosphorus by the Alkalimetric Method

 (0.01 % to 0.05 %)

136-143

Phosphorus by the Molybdenum Blue   Spectrophotometric Method

(0.002 % to 0.05 %)

19-29

Silicon by the Gravimetric Method

 (0.10 % to 2.50 %)

45-51

Sulfur by the Gravimetric  Method-Discontinued 1988

29-35

Sulfur by the Combustion-Iodate   Titration Method-Discontinued 2012

36-44

Sulfur by the Chromatographic  Gravimetric Method-Discontinued 1980

109-116

Tin by the Solvent Extraction-  Atomic Absorption Spectrometry Method

(0.002 % to 0.10 %)

152-161

Vanadium by the Atomic  Absorption Spectrometry Method

(0.006 % to 0.15 %)

193-202

1.3Test methods for the determination of carbon and sulfur not included in this standard can be found in Test Methods E1019.

1.4Some of the composition ranges given in 1.1 are too broad to be covered by a single test method and therefore this standard contains multiple test methods for some elements. The user must select the proper test method by matching the information given in the Scope and Interference sections of each test method with the composition of the alloy to be analyzed.

1.5The values stated in SI units are to be regarded as standard.

1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 6 and in special “Warning” paragraphs throughout these test methods.

1.7This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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